D4928
Standard Test Methods for
Water in Crude Oils by Coulometric Karl Fischer Titration


1.1 This test method covers the determination of water in the range from 0.02 to 5 mass or volume % in crude oils. Mercaptan (RSH) and sulfide (S- or H2S) as sulfur are known to interfere with this test method, but at levels of less than 500 ug/g (ppm), the interference from these compounds is insignificant (see Section 5).

1.2 This test method can be used to determine water in the 0.005 to 0.02 mass % range, but the effects of the mercaptan and sulfide interference at these levels has not been determined.

1.3 This test method is intended for use with standard commercially available coulometric Karl Fischer reagent.

 

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