D189

D189-97
Standard Test Method for Conradson Carbon Residue of Petroleum Products

1.1 This test method covers the determination of the amount of carbon residue (Note 1) left after evaporation and pyrolysis of an oil, and is intended to provide some indication of relative coke-forming propensities. This test method is generally applicable to relatively nonvolatile petroleum products which partially decompose on distillation at atmospheric pressure. Petroleum products containing ash-forming constituents as determined by Test Method D-482 or IP Method 4 will have an erroneously high carbon residue, depending upon the amount of ash formed (Notes 2 and 4).

Note 1-The term carbon residue is used throughout this test method to designate the carbonaceous residue formed after evaporation and pyrolysis of a petroleum product. The residue is not composed entirely of carbon, but is a coke which can be further changed by pyrolysis. The term carbon residue is continued in this test method only in deference to its wide common usage. Note 2-Values obtained by this test method are not numerically the same as those obtained by Test Method D-524. Approximate correlations have been derived (see Fig X1.1), but need not apply to all materials which can be tested because the carbon residue test is applied to a wide variety of petroleum products. Note 3-The test results are equivalent to Test Method D-4530, (see Fig. X1.2). Note 4-In diesel fuel, the presence of alkyl nitrates such as amyl nitrate, hexyl nitrate, or octyl nitrate causes a higher residue value than observed in untreated fuel, which can lead to erroneous conclusions as to the coke forming propensity of the fuel. The presence of alkyl nitrate in the fuel can be detected by Test Method D-4046.

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