D92

D7418-07
Standard Practice for Set-Up and Operation of Fourier Transform Infrared (FT-IR) Spectrometers
for In-Service Oil Condition Monitoring

This practice describes to the end user how to collect the FT-IR spectra of in-service oil samples for in-service oil condition monitoring. Various in-service oil condition monitoring parameters, such as oxidation, nitration, soot, water, ethylene glycol, fuel dilution, gasoline dilution, sulfate by-products and phosphate antiwear additives, can be measured by FT-IR spectroscopy (5-8), as described in Practice E 2412. Changes in the values of these parameters over operating time can then be used to help diagnose the operational condition of various machinery and equipment and to indicate when an oil change should take place. This practice is intended to give a standardized configuration for FT-IR instrumentation and operating parameters employed in in-service oil condition monitoring in order to obtain comparable between-instrument and between-laboratory data.

1.1 This practice covers the instrument set-up and operation parameters for using FT-IR spectrometers for in-service oil condition monitoring for both direct trend analysis and differential trend analysis approaches.

1.2 This practice describes how to acquire the FT-IR spectrum of an in-service oil sample using a standard transmission cell and establishes maximum allowable spectral noise levels.

1.3 Measurement and integrated parameters for individual in-service oil condition monitoring components and parameters are not described in this practice and are described in their respective test methods.

REAL Services 700 Portage Trail Cuyahoga Falls, OH 44221.3057

voice: 330.630.3700 fax: 330.630.3733